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Get Free AccessThe absolute and relative configurations of 1-epialexine are established by X-ray crystallographic analysis, giving (1S,2R,3R,7S,7aS)-1,2,7-trihydroxy-3-(hydroxymethyl)pyrrolizidine. The compound crystallizes as the hemihydrate C8H15NO4·0.5H2O, with hydrogen bonds holding the water molecule in a hydrophilic pocket between epialexine bilayers. In addition, a comparison was made between results obtained from examination of the Bijvoet pairs from data sets collected using molybdenum and copper radiation.
Amber L. Thompson, D.J. Watkin, Zoltán A. Gál, Laurence Jones, Jackie Hollinshead, Sarah F. Jenkinson, George W. J. Fleet, Robert J. Nash (2008). The absolute configuration of 1-epialexine hemihydrate. , 64(12), DOI: https://doi.org/10.1107/s0108270108037086.
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Type
Article
Year
2008
Authors
8
Datasets
0
Total Files
0
Language
en
DOI
https://doi.org/10.1107/s0108270108037086
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