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  5. Synthesis, Structure, and Properties of Mesoporous B/C/N Microspheres

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Article
English
2009

Synthesis, Structure, and Properties of Mesoporous B/C/N Microspheres

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English
2009
Zeitschrift für anorganische und allgemeine Chemie
Vol 636 (1)
DOI: 10.1002/zaac.200900377

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Cnr Rao
Cnr Rao

Jawaharlal Nehru Centre for Advanced Scientific Research

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Kalyan Raidongia
K. P. S. S. Hembram
Umesh V. Waghmare
+2 more

Abstract

Reaction of low surface area carbon with a mixture of urea and boric acid at 930 °C yields a composition close to BC 4 N with a graphitic structure. BC 4 N was characterized by electron energy loss spectroscopy, X‐ray photoelectron spectroscopy, transmission electron microscopy, Raman spectroscopy, and X‐ray diffraction. BC 4 N is a porous ceramic with a surface area of 428 m 2 · g –1 , and shows a CO 2 uptake of 40 wt‐%. The layered structure of BC 4 N involves a random distribution of boron, carbon, and nitrogen atoms and shows high thermal stability up to 1000 °C. A comparative analysis of the structure and properties of BC 4 N and graphene using first‐principles pseudopotential based density functional theoretical calculations is presented. The calculations predict it to be an insulator. The bulk modulus of BC 4 N exhibits an interesting dependence on the ordering of boron and nitrogen on the graphene lattice.

How to cite this publication

Kalyan Raidongia, K. P. S. S. Hembram, Umesh V. Waghmare, Muthusamy Eswaramoorthy, Cnr Rao (2009). Synthesis, Structure, and Properties of Mesoporous B/C/N Microspheres . Zeitschrift für anorganische und allgemeine Chemie, 636(1), pp. 30-35, DOI: 10.1002/zaac.200900377.

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Publication Details

Type

Article

Year

2009

Authors

5

Datasets

0

Total Files

0

Language

English

Journal

Zeitschrift für anorganische und allgemeine Chemie

DOI

10.1002/zaac.200900377

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